Certified Chemistry Laboratory
Lab Brochure (Adobe PDF)
Laboratory
Capabilities
PELA operates
a full service analytical environmental laboratory. PELA's
certified chemistry laboratory has an approved Comprehensive
Quality
Assurance Plan with the following capabilities:
- Safe
Drinking Water Act, 40 CFR, Part 141 & 143
- Drinking
Water Analysis 62-550
- EPA
Priority Pollutants
- Waste
Water Analysis
- NPDES, 40
CFR Part 122
- Haz. Waste
Characterization, 40 CFR part 261. [TCLP, reactivity,
ignitability]
- Underground
Storage Tank Testing 17-770
- RCRA
Compliance Testing SW-846
The
laboratory analyzes solids and liquids for a variety of
organic, inorganic, bacteriological, and radiological
parameters.
Analytical
Quality Control...Precision and Accuracy
PELA's
laboratory personnel are dedicated to maintenance of quality
control programs that assure the highest possible degree of
accuracy
and precision. Procedures and results are routinely checked
and verified
against standards from the U.S. Environmental Protection
Agency (EPA),
National Bureau of Standards (NBS), and U.S. Geological Survey
(USGS).
Stringent compliance criteria for quality control are
performed on a quarterly
basis. Quality control is an integral part of PELA's
laboratory routine.
A routine quality assurance program is an essential part of
the analytical process. The minimum requirements for each
analytical run are as follows:
- Calibration,
Initial & Verification:
A series of four standards are utilized to initiate any
type of analysis.
- Continuing
Calibration Verification:
An EPA quality control check sample or an NBS Control
standard is analyzed every ten samples to assure
calibration accuracy during an analytical run.
- Method
Blank Analysis:
The method blank is to control any contamination from
reagent or preparation.
- Matrix
Spike Analysis:
For each group of ten samples or less of a similar matrix,
a spike sample analysis is performed.
- Duplicate
Sample Analysis:
At least one duplicate sample analysis is performed on
each group of ten samples of a similar matrix.
- GC/MS
Requirements:
DFTPP is verified prior to all analysis
Laboratory
Affiliations and Certifications Include:
- USEPA
- ASTM
- USGS
- USOSM
- Florida
Department of Health and Rehabilitative Services
- Alabama
Department of Environmental Management
- Five
Florida Water Management Districts
- Tennessee
Department of Health and Environment
- Kentucky
Department for Environmental Protection
- Georgia
Department of Natural Resources
Instrumentation-Partial
Equipment List
- Inductively
Coupled Plasma Emission Spectrometer (ICP)
- Flame
Atomic Absorption Spectrometer (FAA)
- Graphite
Furnace Atomic Absorption (GFAA)
- Mercury
Auto Analyzer
- Organic
Carbon Analyzer (TOC)
- Alpkem
Auto Analyzer
- High
Performance Liquid Chromatograph (HPLC)
- Gas
Chromatographs (GC) with different detectors
- Electron
Capture Detector (ECD)
- Flame
Ionization Detector (FID)
- Electrolytic
Conductivity Detector (Hall)
- Nitrogen
Phosphorus Detector (NPD)
- Photoionization
Detector (PID)
- Closed
System Purge and Trap
- GC/Mass
Spectrometer (GC/MS)
The HPLC and
Gas Chromatographs are interlinked to the Turbochrom
Chromatography Computer System. This system calibrates and
processes the chromatographic data for the GC instruments to
be ready for final reporting. PELA is managing laboratory data
within an information management structure by the
implementation of Analytical Automation Specialists, Inc.
LABWORKS LIMS. All instrumentations are interfaced with the
LIMS for Good Automated Laboratory Procedure (GALP) and
automated data collection.
Senior chemists with years of experience in analytical,
physical, and research
chemistry, as well as geochemistry and biochemistry, directly
supervise all work in PELA's laboratory. Strict adherence to
company Standard Operating Procedures
for Quality Assurance/Quality Control is maintained at all
times.
Standard-Turn-Around
A
standard-turn-around-time of three weeks or less (routinely
ten working days) is provided in performing laboratory
analyses for samples collected by PELA's professionals. A turn
around time of 24 hours is available by special request.
Monitoring programs are designed for specific requirements.
The monitoring is performed on a regular basis for government,
industries, and individuals. Personnel
are completely familiar with the use of specialized sampling
devices and proper procedures for collecting corrosive,
ignitable, radioactive, or other hazardous
materials.
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